Laboratory 2
Rocks and Minerals Laboratory

Pamela J. W. Gore

Department of Geology, Georgia Perimeter College

Clarkston, GA 30021

Copyright © 1998-2009 Pamela J. W. Gore

See newer version of this page at http://facstaff.gpc.edu/~pgore/geology/historical_lab/Rocks_and_Minerals.pdf

In this lab you will learn about rocks and minerals. Minerals are the building blocks of rocks, and rocks are the building blocks of the Earth's crust. This lab will introduce you to some of the major rock-forming minerals, and to the three major groups of rocks - igneous, sedimentary and metamorphic. This course will go into more detail with sediments and sedimentary rocks in later labs because it is the sedimentary rocks which record the history of life on Earth. We can also learn to "read the rock layers" to learn many things about the conditions on Earth in the far geologic past, such as ancient climates, tectonic settings, and depositional environments.

BASIC DEFINITIONS

Minerals

Minerals are:

  1. Naturally occurring
  2. Inorganic
  3. Solids
  4. Minerals have a definite chemical composition
  5. Minerals have an orderly internal crystal structure

Minerals are the building blocks of rocks. Each mineral has different physical and chemical properties which allow it to be identified. Physical properties you will use to identify the minerals include color, hardness, luster, cleavage, magnetism, reaction to acid, etc.

Rocks

An aggregate of one or more minerals. Rocks are the building blocks of the Earth's crust. The Earth's continental crust is dominated by granite, and the oceanic crust is dominated by basalt. Both of these are igneous rocks.

There are three basic categories of rocks:

  • Igneous (or crystallized from hot lava or magma) - ex. granite, basalt
  • Sedimentary (or fragments laid down by water or wind) - ex. sandstone, shale, limestone
  • Metamorphic (or rocks changed by heat and or pressure) - ex. gneiss, schist, slalte, marble

Physical Properties of Minerals

  1. Color - The color of the mineral as it appears in reflected light to the naked eye.

  2. Luster - The character of the light reflected from the mineral. A mineral may have a metallic luster (in other words, you would call it a metal), or a non-metallic luster. Non-metallic lusters may be described in more detail as:

     

    glassy or vitreous

    dull

    pearly

    resinous

    waxy

    adamantine

    silky

     

  3. Hardness - The resistanceof a mineral to scratching. Hardness is measured on a scale of 1-10 called Mohs Hardness Scale. In lab, we express hardness in comparison to common objects (fingernail, copper penny, nail, glass).

     

    1. Talc
    2. Gypsum
      ________ fingernail
    3. Calcite
      ________ penny (copper)
    4. Fluorite
      _________ nail
    5. Apatite
      _________ glass
    6. Orthoclase feldspar (K feldspar)
    7. Quartz
    8. Topaz
    9. Corundum
    10. Diamond

       

  4. Cleavage - the tendency of a mineral to break along flat surfaces related to planes of weakness in its crystal structure. Minerals can be identified by the number of cleavage planes they exhibit, and the angles between them. For example, some minerals tend to cleave or break into flat sheets (the micas: muscovite and biotite), other break into cubes (halite), or into rhombs (calcite and dolomite). Other minerals have different types of cleavage. For purposes of this lab, it will be necessary to recognize whether or not minerals have cleavage, and to tell if the cleavage is one of the types mentioned above. For more specific information on cleavage and photographs, see the Physical Geology web page on Minerals. http://facstaff.gpc.edu/~pgore/geology/geo101/mineral.htm

  5. Fracture - irregular breakage not related to planes of weakness in the mineral. Some minerals, such as quartz and olivine do not have cleavage. They have instead a special type of breakage called conchoidal fracture. Conchoidal fracture produces curved breakage surfaces, such as would be seen on arrowheads or chipped glass.

  6. Magnetism - A few minerals are magnetic - that is, they are attracted to a magnet, or they act as a natural magnet, attracting small steel objects such as paperclips. The only magnetic mineral we may see in lab is magnetite.

  7. Reaction to acid - The carbonate minerals react with dilute hydrochloric acid (HCl) by fizzing, producing bubbles of carbon dioxide gas (the same type of harmless gas bubbles that are found in carbonated beverages). Calcite fizzes readily in hydrochloric acid. Dolomite will fizz if it is first scratched and powdered. You may use a nail or steel needle probe to scratch the specimen to try this test.

    If you are taking the course online, you will need to borrow a small amount of HCL acid from the lab, or you may try to obtain it locally. It is sold in some hardware stores as muriatic acid. It may also be available from some pharmacies. If you decide to obtain your own acid locally, please be careful with the acid as it is hazardous and may cause acid burns to the skin or eyes, and will burn holes through clothing. You should wear goggles and rubber gloves when handling it outside of the lab. Use a dropper bottle, and only apply one or two small drops to the sample, and examine it carefully to look for tiny gas bubbles. If the mineral is calcite, you will see them right away. Please remember that acid is a hazardous material and follow any package directions carefully. If you obtain and use hydrochloric acid at home, you are responsible for it, not Georgia Perimeter College.

    Also note that it is NOT necessary for online students to use the acid. If you wish to know whether a particular sample would fizz in acid, you may e-mail the instructor to find out whether or not it will fizz.






IDENTIFYING MINERALS

Use the table below or information in your textbook to identify minerals in the lab.






















Mineral

Color

Hardness

Luster

Cleavage

Reaction to HCl acid

Silicate Minerals

Quartz

Colorless, gray, white

H>glass

Glassy

No cleavage. Has conchoidal fracture

--

Feldspar

White, pink, gray, green 

H>glass

Nonmetallic

Has cleavage

--

Olivine

Olive green

H>glass 

Glassy

No cleavage. Has conchoidal fracture

--

Muscovite

Silvery

H<fingernail 

Nonmetallic

Splits into flat sheets

--

Biotite

Brown to black

fingernail<H<penny 

Nonmetallic, glassy

Splits into flat sheets

--

Pyroxene

Green to black

H<nail 

Nonmetallic

Has cleavage

--

Amphibole

Green to black

H<nail 

Nonmetallic

Has cleavage

--

Garnet

Dark red

H>glass

Nonmetallic

No cleavage

--

Clay minerals

Variable, such as white, orange

H<fingernail

Dull luster

Cleavage not visible to naked eye

--

Carbonate Minerals

Calcite

White, tan, gray, black, etc.

fingernail<H<penny 

Nonmetallic

Has cleavage. Breaks into rhombs

Fizzes readily

Dolomite

White, tan, gray, black, etc.

penny<H<nail 

Nonmetallic

Has cleavage. Breaks into rhombs

Fizzes if scratched and powdered

Other mineral groups

Gypsum

Usually white

H<fingernail 

Nonmetallic

Has cleavage. May break into fibers or flat sheets.

--

Halite

Colorless to white or gray

fingernail<H<penny 

Nonmetallic

Has cleavage. Breaks into cubes

--

 Magnetite

 

 H>glass

Submetallic to metallic 

No cleavage

 

Mineral images

Quartz (crystals)

Potassium feldspar

Olivine

Muscovite

Biotite

Pyroxene

Calcite

Halite

IGNEOUS ROCKS

Igneous rocks are "fire-formed". They crystallized from hot, molten lava or magma as it cooled. Magma is hot, molten rock beneath the surface of the Earth. Lava is hot, molten rock which has flowed out onto the surface of the Earth. Magma may cool within the earth's crust to form igneous rocks. But lava cools much more quickly because it is on the Earth's surface where temperatures are much lower than they are at depth.

Cooling rates influence the texture of the igneous rock:

  • Quick cooling = fine grains
  • Slow cooling = coarse grains

Igneous rocks are classified or named based on their texture and their composition. A variety of textures are present in igneous rocks. For this lab, we will only consider a few: fine-grained (aphanitic), coarse-grained (phaneritic), glassy, and vesicular.

Igneous rock textures

  1. Glassy - instantaneous cooling
    • Obsidian = volcanic glass
    • Obsidian

  2. Aphanitic - fine grain size (< 1 mm); result of quick cooling
  3. Rhyolite

    • Basalt
    • Rhyolite
    • Andesite

  4. Phaneritic - coarse grain size; visible grains (1-10 mm); result of slow cooling
  5. Granite - polished

    • Granite
    • Diorite
    • Gabbro

  6. Vesicular - contains tiny holes called vesicles which formed due to gas bubbles in the lava or magma. Very porous. May resemble a sponge. Commonly low density; may float on water.
    • Vesicular basalt - basalt with a vesicles, which may be quite large. Sometimes lined with crystals to form geodes.
    • Vesicular basalt


      Vesicular basalt with olivine phenocrysts, building stone at Hawaiian Volcano Observatory, Big Island of Hawaii

    • Pumice - light in color; white to gray; may be glassy or dull. Fully riddled with holes. Very sponge-like. Floats. Used as an abrasive. (Pumice stone, Lava Soap).
    • Pumice


Composition of Igneous Rocks

Igneous rocks can be classified into four groups based on their chemical compositions:

  1. Sialic (or granitic or felsic)
    1. Dominated by silicon and aluminum (SiAl)
    2. Usually light in color
    3. Characteristic of continental crust
    4. Forms a stiff (viscous) lava or magma
    5. Rock types include:
      1. Granite
      2. Granite

      3. Rhyolite
      4. Rhyolite

    6. Minerals commonly present include:
      1. potassium feldspar (generally pink or white)
      2. Na-plagioclase feldspar (generally white)
      3. quartz (generally gray or colorless)
      4. biotite
      5. amphibole?
      6. muscovite?

  2. Intermediate (or andesitic)
    1. Intermediate in composition between sialic and mafic
    2. Rock types include:
      1. Andesite (aphanitic)
      2. Diorite (phaneritic)

      Diorite

    3. Minerals commonly present include:
      1. plagioclase feldspar
      2. amphibole
      3. pyroxene
      4. biotite
      5. quartz

  3. Mafic (or basaltic)
    1. Contains abundant ferromagnesian minerals (magnesium and iron silicates)
    2. Usually dark in color (dark gray to black)
    3. Characteristic of Earth's oceanic crust, Hawaiian volcanoes
    4. Forms a runny (low viscosity) lava
    5. Also found on the Moon, Mars, and Venus
    6. Rock types include:
      1. Basalt (aphanitic)
      2. Basalt

      3. Gabbro (phaneritic)
      4. Gabbro

  4. Ultramafic
    1. Almost entirely magnesium and iron silicates (ferromagnesian minerals)
    2. Rarely observed on the Earth's surface
    3. Believed to be major constituent of Earth's mantle
    4. Commonly found as xenoliths in basaltic lavas
    5. Rock types include:
    6. Peridotite (phaneritic) - dominated by olivine - the birthstone is Peridot, which gives its name to Peridotite

      Peridotite

    7. Minerals commonly present include:
      1. Olivine is dominant. (Olivine is olive green).
      2. may have minor amounts of pyroxene and Ca-plagioclase


Igneous Rock Classification Chart

Composition

Texture

Sialic

Intermediate

Mafic

Ultramafic

Fine-grained (aphanitic)

 Rhyolite

Andesite

Basalt

--------------

Coarse-grained (phaneritic)

 Granite

Diorite

Gabbro

Peridotite

Use this chart to name the igneous rocks. Determine the texture and the composition of the sample, and then read its name from the classification chart. Other igneous rocks which you may see in lab, but which are not on this chart are obsidian and pumice.

SEDIMENTARY ROCKS

Sedimentary rocks are made from sediment. Sediment is loose particulate material (clay, sand, gravel, etc.)

Sediment becomes sedimentary rock through lithification, which involves:

  1. Compaction
  2. Cementation
  3. Recrystallization (of carbonate sediment)

Types of sedimentary rocks

A. Terrigenous (also called detrital or clastic) Terrigenous sedimentary rocks are derived from the weathering of pre-existing rocks. They have a clastic (broken or fragmental) texture consisting of:

  1. Clasts (larger pieces, such as sand or gravel)
  2. Matrix (mud or fine-grained sediment surrounding the clasts)
  3. Cement (the glue that holds it all together), such as:
    1. calcite - fizzes in HCl acid
    2. iron oxide - reddish brown color
    3. silica - neither fizzes nor is reddish brown

Clasts and matrix (labelled),
and iron oxide cement
(reddish brown color)

Terrigenous sedimentary rocks are classified according to their texture (grain size):

  • Gravel: Grain size greater than 2 mm
    • If rounded clasts = conglomerate
    • If angular clasts = breccia
    • Conglomerate Breccia


  • Sand: Grain size 1/16 to 2 mm
    • Sandstone is most commonly made of quartz and feldspar, but it may contain grains of nearly any mineral composition, and also grains of fine-grained rock types (such as basalt).
    • If dominated by quartz grains = quartz sandstone (also called quartz arenite)
    • If dominated by feldspar grains = arkose
    • If dominated by rock fragment grains = lithic sandstone (also called litharenite or graywacke)
    • Quartz Sandstone

      Arkose

      Graywacke (lithic sandstone)


  • Silt: Grain size 1/256 to 1/16 mm (gritty)
    • Siltstone
    • Siltstone


  • Clay: Grain size less than 1/256 mm (smooth)
    • Shale (if fissile)
    • Claystone (if massive)

    • Note: Mud is technically a mixture of silt and clay. It forms a rock called mudstone (or mudshale if fissile).

      Shale - fissile
      Claystone
      (kaolinite)
      - not fissile


B. Chemical/biochemical Sedimentary Rocks

This group includes the evaporites, the carbonates (limestones and dolostone), and the siliceous rocks.

These rocks form within the depositional basin from chemical components dissolved in the seawater. These chemicals may be removed from seawater and made into rocks by chemical processes, or with the assistance of biological processes (such as shell growth). In some cases it is difficult to sort the two out (in carbonates or some siliceous rocks, for example), so they are grouped together as chemical/biochemical.

  1. Evaporites - The evaporites form from the evaporation of water (usually seawater).
    1. Rock salt - composed of halite (NaCl).
    2. Rock gypsum - composed of gypsum (CaSO4.2H20)
    3. Travertine - composed of calcium carbonate (CaCO3), and therefore, also technically a carbonate rock; travertine forms in caves and around hot springs.
    Layered gypsum of the Castille Formation,
    Carlsbad, New Mexico
    Gypsum crystals, Marion lake,
    Australia


  2. Carbonates - The carbonate sedimentary rocks are formed through both chemical and biochemical processes. They include the limestones (many types which you will learn about in a later lab) and dolostones.
  3. Two minerals are dominant in carbonate rocks:

    1. Calcite (CaCO3)
    2. Dolomite (CaMg(CO3)2)
    3. li>Remember which of these fizzes readily, and which of these must be scratched or powdered!

  4. Siliceous rocks - The siliceous rocks are those which are dominated by silica (SiO2). They commonly form from silica-secreting organisms such as diatoms, radiolarians, or some types of sponges (you will learn about these in later labs).
    1. Diatomite - looks like chalk, but does not fizz in acid. Made of microscopic planktonic organisms called diatoms. May also resemble kaolinite, but is much lower in density and more porous). Also referred to as Diatomaceous Earth.
    2. Chert - Massive and hard, microcrystalline quartz. May be dark or light in color. Often replaces limestone. Does not fizz in acid.

C. Organic Sedimentary Rocks (Coals)

This group consists of rocks composed of organic matter (mainly plant fragments). Because of this, they lack minerals (which must be inorganic, be definition). These are the coals. There are several types of coal, which you will learn about in a later lab.

METAMORPHIC ROCKS

Metamorphism causes changes in the texture and mineralogy of other rocks.

Texture
The processes of compaction and recrystallization change the texture of rocks during metamorphism.

  1. Compaction
    • The grains move closer together.
    • The rock becomes more dense.
    • Porosity is reduced.
    • Example: clay to shale to slate

  2. Recrystallization
    Growth of new crystals. No changes in overall chemistry. New crystals grow from the minerals already present.

    A preferred orientation of minerals commonly develops under applied pressure. Platy or sheet-like minerals such as muscovite and biotite become oriented perpendicular to the direction of force. This preferred orientation is called foliation.


Metamorphic Textures

  • Foliation is a broad term referring to the alignment of sheet-like minerals. Examples: slate, phyllite, schist, gneiss.
  • Non-foliated or granular metamorphic rocks are those which are composed of equidimensional grains such as quartz or calcite. There is no preferred orientation. The grains form a mosaic. Examples: quartzite and marble.

    Note: Not all quartzites and marbles are pure. Some contain impurities that were originally mud interlayered with or mixed with the original quartz sand or lime mud. These clay impurities metamorphose to layers of micas or other minerals, which may give marble (in particular) a banded, gneissic appearance, or which may give a slight foliation to some quartzites.

The foliated metamorphic rocks As shale is subjected to increasing grade of metamorphism (increasing temperatures and pressures), it undergoes successive changes in texture associated with an increase in the size of the mica grains.

  1. Slate - very fine grained rock. Resembles shale. Has slaty cleavage which may be at an angle to the original bedding. Relict bedding may be seen on cleavage planes. Often dark gray in color. "Rings" when you strike it. (Unlike shale, which makes a dull sound. Temperature about 200 degrees C; Depth of burial about 10 km.


  2. Phyllite - fine-grained metamorphic rock. Has a frosted sheen, resembling frosted eye shadow. This is no coincidence. Cosmetics commonly contain ground up muscovite (ground to a size similar to that occurring naturally in phyllite.)


  3. Schist - metamorphic rock containing abundant obvious micas, several millimeters across. Several types of schist may be recognized, based on minerals which may be present:
    • mica schist
    • garnet schist
    • chlorite schist
    • kyanite schist
    • talc schist


  4. Gneiss - (pronounced "nice") - a banded or striped rock with alternating layers of dark and light minerals. The dark layers commonly contain biotite, and the light layers commonly contain quartz and feldspar.


The non-foliated (and weakly foliated) metamorphic rocks

  1. Marble - fizzes in acid because its dominant minerals is calcite (or dolomite). The parent rock is limestone (or dolostone).


  2. Quartzite - interlocking grains of quartz. Scratches glass. The rock fractures through the grains (rather than between the grains as it does in sandstone). The parent rock is quartz sandstone.

  3. Greenstone - dark green rock with very fine texture. May contain chlorite and may be slightly foliated. The parent rock is basalt.


Formation of new minerals - there are a number of metamorphic minerals which form during metamorphism and are found exclusively (or almost exclusively) in metamorphic rocks:

  • Garnet - dark red dodecahedrons (12 sides)
  • Staurolite - brown lozenge-shaped minerals, commonly twinned to form "fairy crosses". State mineral of Georgia.

  • Kyanite - sky blue bladed minerals with differential hardness. Scratch lengthwise with a knife or nail, but not sideways.

  • Chlorite - dark bluish green, soft. Fe, Mg
  • Talc - white or pale green and soft.
  • Graphite - metamorphosed carbon
  • Tourmaline - commonly black. Forms elongated crystals with a rounded triangular cross-section.
  • Micas - muscovite (silvery), biotite (dark brown).

Go to Rocks and Minerals - EXERCISES to do lab.

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This page created by Pamela J. W. Gore
Georgia Perimeter College

July 22, 1998
Modified February 26, 1999
Modified June 11, 1999
Links updated December 1, 2003
Image links updated October 28, 2008


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